2,6-Pyridinedicarbonyl dichloride, 4-(phenylmethoxy)-

Base Information

Chemical Name:2,6-Pyridinedicarbonyl dichloride, 4-(phenylmethoxy)-
CAS No.:247576-45-0
Molecular Formula:C14H9Cl2NO3
Molecular Weight:310.136
Hs Code.:
Mol file:247576-45-0.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-Pyridinedicarbonyl dichloride, 4-(phenylmethoxy)-

Chemical Property:

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Technology Process of 2,6-Pyridinedicarbonyl dichloride, 4-(phenylmethoxy)-

There total 8 articles about 2,6-Pyridinedicarbonyl dichloride, 4-(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 486459-27-2
4-benzyloxy-2,6-pyridinedicarboxylic acid

: 247576-45-0
4-benzyloxypyridine-2,6-dicarboxylic acid dichloride

Guidance literature:: With thionyl chloride; In N,N-dimethyl-formamide; at 2 ℃; for 75h;
DOI:10.1016/j.tet.2008.05.075

Reference yield: 73.0%

: C₁₄H₉NO₅^(2-)*2K⁽¹⁺⁾

: 247576-45-0
4-benzyloxypyridine-2,6-dicarboxylic acid dichloride

Guidance literature:: With thionyl chloride; In toluene; for 4.5h; Inert atmosphere; Reflux;
DOI:10.1016/j.molcata.2010.10.023

Reference yield:

: 99097-42-4
4-benzyloxypyridine-2,6-dicarboxylic dimethyl ester

: 247576-45-0
4-benzyloxypyridine-2,6-dicarboxylic acid dichloride

Guidance literature:: 4-benzyloxypyridine-2,6-dicarboxylic dimethyl ester; With potassium hydroxide; In ethanol; for 0.5h; Heating;

With oxalyl dichloride; In benzene; for 4h; Further stages.; Heating;
DOI:10.1002/1521-3765(20021004)8:19<4434::AID-CHEM4434>3.0.CO;2-#