O-<4-Methoxyphenyl>-S--dithiocarbonat

Base Information

• Chemical Name: O-<4-Methoxyphenyl>-S--dithiocarbonat
• CAS No.: 19574-46-0
• Molecular Formula: C₁₀H₁₀ClNOS₃
• Molecular Weight: 291.846

Synonyms:

Chemical Property of O-<4-Methoxyphenyl>-S--dithiocarbonat

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of O-<4-Methoxyphenyl>-S--dithiocarbonat

There total 2 articles about O-<4-Methoxyphenyl>-S--dithiocarbonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thiophosgene (463-71-8) + 4-chloro-phenol (106-48-9,82344-39-6) + sodium dimethyldithiocarbamate (128-04-1) → O-<4-Methoxyphenyl>-S--dithiocarbonat (19574-46-0)

Guidance literature:

Multistep reaction; (i) aq. NaOH, CHCl₃, (ii) /BRN= 3569024/, H₂O;

DOI:10.1246/bcsj.34.254

Reference yield:

→ O-<4-Methoxyphenyl>-S--dithiocarbonat (19574-46-0)

Guidance literature:

(CH3)2N-C(S)-SNa, /BRN= 565729/, Acn.;

DOI:10.1248/yakushi1947.88.2_227

Reference yield:

O-<4-Methoxyphenyl>-S--dithiocarbonat (19574-46-0) → 4-chlorophenyl-O-(N,N-dimethylthiocarbamate) (10345-52-5)

Guidance literature:

(thermolysis);

DOI:10.1246/bcsj.34.254

upstream raw materials:

thiophosgene

4-chloro-phenol

sodium dimethyldithiocarbamate

Downstream raw materials:

4-chlorophenyl-O-(N,N-dimethylthiocarbamate)

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