Technology Process of 1-Hexadecanol, 10-methyl-
There total 1 articles about 1-Hexadecanol, 10-methyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: pyridinium p-toluenesulfonate / dichloromethane
2.1: sodium hydride; diisopropylamine / paraffin oil; tetrahydrofuran / 0 - 60 °C / Inert atmosphere
2.2: 1.3 h / -10 - 30 °C / Inert atmosphere
2.3: 12 h / 28 °C / Inert atmosphere
3.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere; Reflux
4.1: triethylamine / chloroform / 12 h / 20 °C / Cooling with ice
5.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere; Reflux
6.1: pyridinium p-toluenesulfonate; methanol / 4 h / Reflux
With
methanol; lithium aluminium tetrahydride; pyridinium p-toluenesulfonate; sodium hydride; triethylamine; diisopropylamine;
In
tetrahydrofuran; diethyl ether; dichloromethane; chloroform; paraffin oil;
DOI:10.1002/jlcr.3504
- Guidance literature:
-
With
chromium(VI) oxide; sulfuric acid;
In
acetone;
at 0 ℃;
for 3.5h;
DOI:10.1002/jlcr.3504
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 3.5 mg / CrO3 / acetic acid / 2 h / Ambient temperature
2: 3.7 mg / diethyl ether; diethyl ether
With
chromium(VI) oxide;
In
diethyl ether; acetic acid;
DOI:10.1021/jo00053a034