benzyl N-[(benzyloxy)carbonyl]-O-[bis(2-chloropropyl)carbamoyl]serinate

Base Information

• Chemical Name: benzyl N-[(benzyloxy)carbonyl]-O-[bis(2-chloropropyl)carbamoyl]serinate
• CAS No.: 13723-34-7
• Molecular Formula: C₂₅H₃₀Cl₂N₂O₆
• Molecular Weight: 525.429

Synonyms:Carbamicacid, bis(2-chloropropyl)-, ester with N-carboxy-DL-serine dibenzyl ester; NSC156283

Chemical Property of benzyl N-[(benzyloxy)carbonyl]-O-[bis(2-chloropropyl)carbamoyl]serinate

Chemical Property:

• Vapor Pressure: 3.38E-17mmHg at 25°C
• Boiling Point: 658.2°C at 760 mmHg
• Flash Point: 351.9°C
• Density: 1.266g/cm³

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of benzyl N-[(benzyloxy)carbonyl]-O-[bis(2-chloropropyl)carbamoyl]serinate

There total 1 articles about benzyl N-[(benzyloxy)carbonyl]-O-[bis(2-chloropropyl)carbamoyl]serinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phosgene (75-44-5) + N,N-bis(2-chloro-n-propyl)amine (2475-71-0) + 2-benzyloxycarbonylamino-3-hydroxy-propionic acid benzyl ester (40489-45-0,101914-11-8) → N-Benzyloxycarbonyl-O--DL-serin-benzylester (13723-34-7)

Guidance literature:

Multistep reaction; (i), (ii) /BRN= 1736481/;

DOI:10.1039/j39670000592

Reference yield:

N-Benzyloxycarbonyl-O--DL-serin-benzylester (13723-34-7) → O--DL-serin (3830-16-8,13723-01-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1039/j39670000592

upstream raw materials:

phosgene

N,N-bis(2-chloro-n-propyl)amine

2-benzyloxycarbonylamino-3-hydroxy-propionic acid benzyl ester

Downstream raw materials:

O--DL-serin

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