Pyrimidine, 1,4,5,6-tetrahydro-2-phenyl-

Base Information

Chemical Name:Pyrimidine, 1,4,5,6-tetrahydro-2-phenyl-
CAS No.:25099-77-8
Molecular Formula:C10H12N2
Molecular Weight:160.219
Hs Code.:
Mol file:25099-77-8.mol

Synonyms:2-phenyl-1,4,5,6-tetrahydro-pyrimidine;T0400-2056;2-phenyl-1,3-diazacyclohexene;2-Phenyl-1,4,5,6-tetrahydro-pyrimidin;2-phenyltetrahydropyrimidine;HMS1775H17;2-phenyl-3,4,5,6-tetrahydropyrimidine;1,4,5,6-tetrahydro-2-phenylpyrimidine;HMS2489G09;

Suppliers and Price of Pyrimidine, 1,4,5,6-tetrahydro-2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pyrimidine, 1,4,5,6-tetrahydro-2-phenyl-

Chemical Property:

Melting Point:72-78 °C
Boiling Point:155-165 °C(Press: 5 Torr)
PSA：24.39000
Density:1.09±0.1 g/cm3(Predicted)
LogP:1.19090

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Pyrimidine, 1,4,5,6-tetrahydro-2-phenyl-

There total 29 articles about Pyrimidine, 1,4,5,6-tetrahydro-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 2055-46-1
3,4,5,6-tetrahydropyrimidine-2-thione

: 98-80-6
phenylboronic acid

: 25099-77-8
2-phenyl-1,4,5,6-tetrahydropyrimidine

Guidance literature:: With copper(I)-thiophene-2-carboxylate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 100 ℃; for 1h; under 1500.15 - 2250.23 Torr; microwave irradiation;
DOI:10.1021/jo070408f

Reference yield: 95.0%

: 591-50-4
iodobenzene

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 109-76-2,54018-94-9
Trimethylenediamine

: 25099-77-8
2-phenyl-1,4,5,6-tetrahydropyrimidine

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate; In toluene; for 16h; Inert atmosphere; Reflux;
DOI:10.1021/jo400252n