Ethenesulfonamide, N,N-bis(phenylmethyl)-

Base Information

Chemical Name:Ethenesulfonamide, N,N-bis(phenylmethyl)-
CAS No.:2525-74-8
Molecular Formula:C16H17NO2S
Molecular Weight:287.382
Hs Code.:
Mol file:2525-74-8.mol

Synonyms:

Suppliers and Price of Ethenesulfonamide, N,N-bis(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 8 raw suppliers

Chemical Property of Ethenesulfonamide, N,N-bis(phenylmethyl)-

Chemical Property:

Purity/Quality:: ≥95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Ethenesulfonamide, N,N-bis(phenylmethyl)-

There total 1 articles about Ethenesulfonamide, N,N-bis(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1622-32-8
2-Chloroethanesulfonyl chloride

: 103-49-1
dibenzylamine

: 2525-74-8
N,N-dibenzylethenesulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1021/acs.orglett.9b02867

Reference yield: 38.0%

: 875056-38-5
2-chloro-4-(4,4-dimethyl-5-oxo-2-thioxoimidazolidin-1-yl)benzonitrile

: 2525-74-8
N,N-dibenzylethenesulfonamide

: 875056-39-6
C₂₈H₂₇ClN₄O₃S₂

Guidance literature:: With potassium carbonate; In 1,3-dimethyl-2-imidazolidinone; at 100 ℃; for 7h;

Reference yield:

: 2525-74-8
N,N-dibenzylethenesulfonamide

: 2,N,N-tribenzyl-4-[2-(phenylsulfonyl)ethyl]-1,2,3,4-tetrahydroisoquinoline-4-sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 24 h / Reflux; Inert atmosphere

2: potassium carbonate; lithium iodide / acetonitrile / 24 h / Reflux; Inert atmosphere

3: caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 72 h / 120 °C / Sealed tube; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; caesium carbonate; lithium iodide; In tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1002/ejoc.201601300