Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂)

Base Information

Chemical Name:Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂)
CAS No.:110777-91-8
Molecular Formula:C₂₆H₃₃MoO₄P₃S
Molecular Weight:630.473
Hs Code.:

Mo(CO)2(P(CH<sub>3</sub>)2(C<sub>6</sub>H<sub>5</sub>))3(SO<sub>2</sub>)

Synonyms:

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Chemical Property of Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂)

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Technology Process of Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂)

There total 3 articles about Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84500-97-0,84501-08-6
cis-acetonitriledicarbonyl-bis(triphenylphosphane)(η2-sulfurdioxide)molybdenum

: 672-66-2
Dimethyl(phenyl)phosphine

: 110777-91-8
Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂)

: 110777-91-8
Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂)

: 110777-91-8
Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂)

Guidance literature:: In tetrahydrofuran; addn. of Mo(CO)2(PPh3)2(MeCN)(η2-SO2) to a soln. of PMe2Ph in THF, stirring overnight at room temp., after filtration over Celite the soln.was concd., addn. of ether, pptn. of an orange powder; performed under N2;; washed with ether, dried in vac. (yield 34%:2/1 mixture of trans/cis-COη1-SO2 isomers); mother-liquor cooled to -20°C, ppt. filtered off, washed with hexane, dried (yield 31%:1/1 mixture of cis-CO η1- and η2-SO2 isomer); elem. anal.;

Reference yield:

: 84500-97-0,84501-08-6
cis-acetonitriledicarbonyl-bis(triphenylphosphane)(η2-sulfurdioxide)molybdenum

: 672-66-2
Dimethyl(phenyl)phosphine

: 110777-91-8
Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂)

: 110777-91-8
Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂)

: 110777-91-8
Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂)

Guidance literature:: In tetrahydrofuran; addn. of Mo(CO)2(PPh3)2(MeCN)(η2-SO2) to a soln. of PMe2Ph in THF, stirring overnight at room temp., after filtration over Celite the soln.was concd., addn. of ether, pptn. of an orange powder; performed under N2;; washed with ether, dried in vac. (yield 34%:2/1 mixture of trans/cis-COη1-SO2 isomers); mother-liquor cooled to -20°C, ppt. filtered off, washed with hexane, dried (yield 31%:1/1 mixture of cis-CO η1- and η2-SO2 isomer); elem. anal.;

Reference yield:

: 84500-97-0,84501-08-6
cis-acetonitriledicarbonyl-bis(triphenylphosphane)(η2-sulfurdioxide)molybdenum

: 672-66-2
Dimethyl(phenyl)phosphine

: 110777-91-8
Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂)

: 110777-91-8
Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂)

: 110777-91-8
Mo(CO)2(P(CH₃)2(C₆H₅))3(SO₂)

Guidance literature:: In tetrahydrofuran; addn. of Mo(CO)2(PPh3)2(MeCN)(η2-SO2) to a soln. of PMe2Ph in THF, stirring overnight at room temp., after filtration over Celite the soln.was concd., addn. of ether, pptn. of an orange powder; performed under N2;; washed with ether, dried in vac. (yield 34%:2/1 mixture of trans/cis-COη1-SO2 isomers); mother-liquor cooled to -20°C, ppt. filtered off, washed with hexane, dried (yield 31%:1/1 mixture of cis-CO η1- and η2-SO2 isomer); elem. anal.;