Zn(II)-5-[1,5-bis(dibenzyloxyphosphoryloxy)pent-3-yl]-15-phenylporphyrin

Base Information

Chemical Name:Zn(II)-5-[1,5-bis(dibenzyloxyphosphoryloxy)pent-3-yl]-15-phenylporphyrin
CAS No.:1021946-34-8
Molecular Formula:C₅₉H₅₂N₄O₈P₂Zn
Molecular Weight:1072.42
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Zn(II)-5-[1,5-bis(dibenzyloxyphosphoryloxy)pent-3-yl]-15-phenylporphyrin

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Technology Process of Zn(II)-5-[1,5-bis(dibenzyloxyphosphoryloxy)pent-3-yl]-15-phenylporphyrin

There total 1 articles about Zn(II)-5-[1,5-bis(dibenzyloxyphosphoryloxy)pent-3-yl]-15-phenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 911467-59-9
bis[(propylimino)methyl]dipyrromethane

: 1021946-30-4
5-[1,5-bis(dibenzyloxyphosphoryloxy)pent-3-yl]dipyrromethane

: 557-34-6
zinc diacetate

: 1021946-34-8
Zn(II)-5-[1,5-bis(dibenzyloxyphosphoryloxy)pent-3-yl]-15-phenylporphyrin

Guidance literature:: In toluene; soln. of dipyrromethane-alkyldiphosphate and bis((propylimino)methyl)dipyrromethane in toluene treated with Zn acetate (10 equiv.); reflixed in air for 4.5 h; cooled to room temp.; diluted in CH2Cl2; soln. washed with H2O and brine; org. layer sepd.; dried (Na2SO4); concd. to dryness; chromd. (silica, CH2Cl2-ethyl acetate 4:1); chromd. (silica, hexanes-ethyl acetate 2:3);
DOI:10.1039/b714127k