Butanoic acid, 4-[[4-[[(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1H-pyrazol-4-yl)amino] sulfonyl]phenyl]amino]-4-oxo-

Base Information

Chemical Name:Butanoic acid, 4-[[4-[[(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1H-pyrazol-4-yl)amino] sulfonyl]phenyl]amino]-4-oxo-
CAS No.:253605-53-7
Molecular Formula:C21H22N4O6S
Molecular Weight:458.48800
Hs Code.:
Mol file:253605-53-7.mol

Synonyms:

Suppliers and Price of Butanoic acid, 4-[[4-[[(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1H-pyrazol-4-yl)amino] sulfonyl]phenyl]amino]-4-oxo-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Butanoic acid, 4-[[4-[[(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1H-pyrazol-4-yl)amino] sulfonyl]phenyl]amino]-4-oxo-

Chemical Property:

PSA：147.88000
LogP:3.31530

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Butanoic acid, 4-[[4-[[(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1H-pyrazol-4-yl)amino] sulfonyl]phenyl]amino]-4-oxo-

There total 4 articles about Butanoic acid, 4-[[4-[[(2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1H-pyrazol-4-yl)amino] sulfonyl]phenyl]amino]-4-oxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 108-30-5
succinic acid anhydride

: 71119-16-9
1-phenyl-2,3-dimethyl-4-(4'-aminophenyl)sulfonylamino-5-pyrazolone

: 253605-53-7
3-({4-[(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)sulfamoyl]phenyl}carbamoyl)propanoic acid

Guidance literature:: In 1,4-dioxane; for 5h; Heating;
DOI:10.1007/BF02509936

Reference yield:

: 83-07-8
4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one

: 253605-53-7
3-({4-[(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)sulfamoyl]phenyl}carbamoyl)propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / triethylamine / acetonitrile / 1 h / 20 °C

2: 93 percent / KOH / methanol / 1.5 h / 85 °C

3: 95 percent / dioxane / 5 h / Heating

With potassium hydroxide; triethylamine; In 1,4-dioxane; methanol; acetonitrile; 1: Substitution / 2: Deacetylation / 3: Acylation;
DOI:10.1007/BF02509936

Reference yield:

: 32061-15-7
1-phenyl-2,3-dimethyl-4-(4'-acetylaminophenyl)sulfonylamino-5-pyrazolone

: 253605-53-7
3-({4-[(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)sulfamoyl]phenyl}carbamoyl)propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / KOH / methanol / 1.5 h / 85 °C

2: 95 percent / dioxane / 5 h / Heating

With potassium hydroxide; In 1,4-dioxane; methanol; 1: Deacetylation / 2: Acylation;
DOI:10.1007/BF02509936