Phenol, 3-methoxy-2-(3-methyl-2-butenyl)-

Base Information

Chemical Name:Phenol, 3-methoxy-2-(3-methyl-2-butenyl)-
CAS No.:25801-53-0
Molecular Formula:C12H16O2
Molecular Weight:192.25400
Hs Code.:
DSSTox Substance ID:DTXSID60473094
Nikkaji Number:J2.548.338C
Mol file:25801-53-0.mol

Synonyms:25801-53-0;Phenol, 3-methoxy-2-(3-methyl-2-butenyl)-;3-METHOXY-2-(3-METHYLBUT-2-EN-1-YL)PHENOL;3-methoxy-2-(3-methylbut-2-enyl)phenol;SCHEMBL8702045;DTXSID60473094

Suppliers and Price of Phenol, 3-methoxy-2-(3-methyl-2-butenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Phenol, 3-methoxy-2-(3-methyl-2-butenyl)-

Chemical Property:

Boiling Point:296.9±25.0 °C(Predicted)
PSA：29.46000
Density:1.024±0.06 g/cm3(Predicted)
LogP:2.90950
XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:192.115029749
Heavy Atom Count:14
Complexity:195

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CCC1=C(C=CC=C1OC)O)C

Technology Process of Phenol, 3-methoxy-2-(3-methyl-2-butenyl)-

There total 11 articles about Phenol, 3-methoxy-2-(3-methyl-2-butenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 340825-70-9
4-[2-(2-tetrahydropyranyloxy)-6-methoxyphenyl]-2-methylbut-2-ene

: 25801-53-0
3-methoxy-2-(3-methylbut-2-enyl)phenol

Guidance literature:: With oxalic acid; In methanol; water; at 20 ℃; for 1h;
DOI:10.1002/1521-4184(200102)334:2<53::AID-ARDP53>3.0.CO;2-C

Reference yield:

: 34191-90-7
1-methoxy-3-(2-methylbut-3-yn-2-yloxy)benzene

: 25801-53-0
3-methoxy-2-(3-methylbut-2-enyl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, quinoline / Pd-BaSO₄ / ethanol

2: PhNEt₂, H₂SO₄ / diethyl ether

With quinoline; sulfuric acid; hydrogen; N,N-diethylaniline; palladium on barium sulfate; In diethyl ether; ethanol;

Reference yield:

: 30778-86-0
1-methoxy-3-tetrahydropyran-2-yloxybenzene

: 25801-53-0
3-methoxy-2-(3-methylbut-2-enyl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: nBuLi / cyclohexane; hexane / 0.5 h / Heating

1.2: 52 percent / cyclohexane; hexane / 2 h / Heating

2.1: 98 percent / oxalic acid / methanol; H₂O / 1 h / 20 °C

With n-butyllithium; oxalic acid; In methanol; hexane; cyclohexane; water;
DOI:10.1002/1521-4184(200102)334:2<53::AID-ARDP53>3.0.CO;2-C