Urea, N-[2,6-bis(1-methylethyl)-4-[(triphenylmethyl)amino]phenyl]-N'-[1-butyl-1, 2-dihydro-4-(3-methoxyphenyl)-2-oxo-1,8-naphthyridin-3-yl]-

Base Information

Chemical Name:Urea, N-[2,6-bis(1-methylethyl)-4-[(triphenylmethyl)amino]phenyl]-N'-[1-butyl-1, 2-dihydro-4-(3-methoxyphenyl)-2-oxo-1,8-naphthyridin-3-yl]-
CAS No.:259225-25-7
Molecular Formula:C51H53N5O3
Molecular Weight:784.014
Hs Code.:
Mol file:259225-25-7.mol

Synonyms:

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Chemical Property of Urea, N-[2,6-bis(1-methylethyl)-4-[(triphenylmethyl)amino]phenyl]-N'-[1-butyl-1, 2-dihydro-4-(3-methoxyphenyl)-2-oxo-1,8-naphthyridin-3-yl]-

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Technology Process of Urea, N-[2,6-bis(1-methylethyl)-4-[(triphenylmethyl)amino]phenyl]-N'-[1-butyl-1, 2-dihydro-4-(3-methoxyphenyl)-2-oxo-1,8-naphthyridin-3-yl]-

There total 8 articles about Urea, N-[2,6-bis(1-methylethyl)-4-[(triphenylmethyl)amino]phenyl]-N'-[1-butyl-1, 2-dihydro-4-(3-methoxyphenyl)-2-oxo-1,8-naphthyridin-3-yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 259225-37-1
2,6-diisopropyl-4-tritylaminoaniline

: 873194-72-0
[1-butyl-4-(3-methoxy-phenyl)-2-oxo-1,2-dihydro-[1,8]naphthyridin-3-yl]-carbamic acid phenyl ester

: 259225-25-7
N-[1-butyl-4-(3-methoxyphenyl)-1,2-dihydro-2-oxo-1,8-naphthyridin-3-yl]-N'-(2,6-diisopropyl-4-tritylaminophenyl)urea

Guidance literature:: With dmap; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmcl.2005.09.056

Reference yield:

: 163704-72-1
4-nitro-2,6-diisopropyl aniline

: 259225-25-7
N-[1-butyl-4-(3-methoxyphenyl)-1,2-dihydro-2-oxo-1,8-naphthyridin-3-yl]-N'-(2,6-diisopropyl-4-tritylaminophenyl)urea

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd/C / methanol / 20 °C

2: Et₃N / CH₂Cl₂ / 20 °C

3: 77 percent / DMAP / dimethylformamide / 20 °C

With dmap; hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.09.056

Reference yield:

: 474328-43-3
N-(2,6-diisopropyl-4-nitrophenyl)-4-methylbenzenesulfonamide

: 259225-25-7
N-[1-butyl-4-(3-methoxyphenyl)-1,2-dihydro-2-oxo-1,8-naphthyridin-3-yl]-N'-(2,6-diisopropyl-4-tritylaminophenyl)urea

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / H₂SO₄ / 3 h / 70 °C

2: H₂ / Pd/C / methanol / 20 °C

3: Et₃N / CH₂Cl₂ / 20 °C

4: 77 percent / DMAP / dimethylformamide / 20 °C

With dmap; sulfuric acid; hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.09.056