Aluminum, 1-hexenylbis(2-methylpropyl)-

Base Information

Chemical Name:Aluminum, 1-hexenylbis(2-methylpropyl)-
CAS No.:26076-75-5
Molecular Formula:C14H29Al
Molecular Weight:224.366
Hs Code.:

Synonyms:

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Chemical Property of Aluminum, 1-hexenylbis(2-methylpropyl)-

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Technology Process of Aluminum, 1-hexenylbis(2-methylpropyl)-

There total 1 articles about Aluminum, 1-hexenylbis(2-methylpropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14343-59-0
1,1-bis(diisobutylaluminium)hexane

: 7517-02-4
isopropoxydiisobutylaluminum

: (((CH₃)2CHCH₂)2Al)CH((CH₂)4CH₃)Al(CH₂CH(CH₃)2)OCH(CH₃)2

: 20259-40-9,26076-75-5
diisobutyl(hex-1-en-1-yl)alane

Guidance literature:: With acetone; In pentane; byproducts: isobutene; Me2CO was dropwise added to soln. of alane (1:1 molar ratio) in pentane at -75°C under N2 atmosphere, mixt. was allowed to warm to room temp., refluxed for 30 min; isobutene evolved was collected in a gas burette and analysed by GLC, solvent from the reaction mixt. was distilled off; hydrolysis of residue observed yielding i-PrOH, i-butanol, i-butane, hexane, and 1-hexene (extrn. with ether and analys by GLC);
DOI:10.1016/0022-328X(87)80320-0

Reference yield: 89.0%

: 26076-75-5
(E)-hex-1-enyldiisobutylaluminum

: 932-87-6
1-Bromo-2-phenylacetylene

: 132699-39-9
oct-3-en-1-yn-1-ylbenzene

Guidance literature:: With bis(triphenylphosphine)nickel(II) chloride; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,2-dimethoxyethane; at 60 ℃; for 5h; Inert atmosphere;
DOI:10.1016/j.tet.2021.132549

Reference yield: 86.0%

: 313343-88-3
1-(bromoethynyl)-4-(trifluoromethyl)benzene

: 26076-75-5
(E)-hex-1-enyldiisobutylaluminum

: 1-(oct-3-en-1-yn-1-yl)-4-(trifluoromethyl)benzene

Guidance literature:: With bis(triphenylphosphine)nickel(II) chloride; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,2-dimethoxyethane; at 60 ℃; for 5h; Inert atmosphere;
DOI:10.1016/j.tet.2021.132549