1,3-Bis(4-methoxyphenyl)-2-propylpropane-1,3-dione

Base Information

Chemical Name:1,3-Bis(4-methoxyphenyl)-2-propylpropane-1,3-dione
CAS No.:263717-49-3
Molecular Formula:C20H22O4
Molecular Weight:326.38600
Hs Code.:
DSSTox Substance ID:DTXSID50442254
Nikkaji Number:J1.826.158H
Wikidata:Q72446299
Mol file:263717-49-3.mol

Synonyms:1,3-bis(4-methoxyphenyl)-2-propylpropane-1,3-dione;263717-49-3;starbld0000124;DTXSID50442254;A5240;1,3-bis(4-methoxyphenyl)-2-propyl-1,3-propanedion;2-Propyl-1,3-bis(4-methoxyphenyl)-1,3-propanedione

Suppliers and Price of 1,3-Bis(4-methoxyphenyl)-2-propylpropane-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1,3-Bis(4-methoxyphenyl)-2-propylpropane-1,3-dione

Chemical Property:

Melting Point:58 °C
Boiling Point:488.8±30.0 °C(Predicted)
PKA:10.16±0.27(Predicted)
PSA：52.60000
Density:1.107
LogP:4.18570
XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:326.15180918
Heavy Atom Count:24
Complexity:368

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC(C(=O)C1=CC=C(C=C1)OC)C(=O)C2=CC=C(C=C2)OC

Technology Process of 1,3-Bis(4-methoxyphenyl)-2-propylpropane-1,3-dione

There total 9 articles about 1,3-Bis(4-methoxyphenyl)-2-propylpropane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1671-76-7
p-Methoxyvalerophenon

: 7464-46-2
p-nitrophenyl p-methoxybenzoate

: 263717-49-3
2-propyl-1,3-bis(4-methoxyphenyl)propane-1,3-dione

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at 20 ℃; for 1.5h;
DOI:10.1021/jm000170m

Reference yield: 63.0%

: 1335135-36-8
C₂₀H₂₄O₄

: 263717-49-3
2-propyl-1,3-bis(4-methoxyphenyl)propane-1,3-dione

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 0 - 20 ℃; for 4h; Inert atmosphere; Molecular sieve;
DOI:10.1039/c1ob05150d

Reference yield:

: 638-29-9
n-valeryl chloride

: 263717-49-3
2-propyl-1,3-bis(4-methoxyphenyl)propane-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃ / 1,2-dichloro-ethane / 0 - 20 °C

2: 76 percent / LHMDS / tetrahydrofuran / 1.5 h / 20 °C

With aluminium trichloride; lithium hexamethyldisilazane; In tetrahydrofuran; 1,2-dichloro-ethane; 1: Friedel-Crafts acylation;
DOI:10.1021/jm000170m