(CH₃O)3C₆H₂CO₂B(C₂H₅)2

Base Information

• Chemical Name: (CH₃O)3C₆H₂CO₂B(C₂H₅)2
• CAS No.: 146681-60-9
• Molecular Formula: C₁₄H₂₁BO₅
• Molecular Weight: 280.129
• Mol file: 146681-60-9.mol

Synonyms:

Chemical Property of (CH₃O)3C₆H₂CO₂B(C₂H₅)2

Chemical Property:

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Technology Process of (CH₃O)3C₆H₂CO₂B(C₂H₅)2

There total 1 articles about (CH₃O)3C₆H₂CO₂B(C₂H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethyl borane (97-94-9) + Eudesmic acid (118-41-2) → (CH3O)3C6H2CO2B(C2H5)2 (146681-60-9)

Guidance literature:

In toluene; addn. of slight molar excess of B(C2H5)3 to carboxylic acid (liq. or dissolved in toluene) placed in a cooled vessel (-80°C); warming slowly to 50-80°C;; removing volatiles under reduced pressure; purification by vac. distn. or crystn. from a non-polar solvent;;

DOI:10.1039/DT9930000047

upstream raw materials:

triethyl borane

Eudesmic acid