10-Methylacridinium Perchlorate

Base Information

• Chemical Name: 10-Methylacridinium Perchlorate
• CAS No.: 26456-05-3
• Molecular Formula: C14H12N.ClO4
• Molecular Weight: 293.707
• Hs Code.: 2933990090
• European Community (EC) Number: 677-513-7
• DSSTox Substance ID: DTXSID90473269
• Mol file: 26456-05-3.mol

Synonyms:10-methylacridinium perchlorate

Chemical Property of 10-Methylacridinium Perchlorate

Chemical Property:

• Melting Point: 247 °C
• PSA: 78.15000
• LogP: 3.03180
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 293.0454856
• Heavy Atom Count: 20
• Complexity: 299

Purity/Quality:

98%,99%, ^*data from raw suppliers

10-Methylacridinium Perchlorate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[N+]1=C2C=CC=CC2=CC3=CC=CC=C31.[O-]Cl(=O)(=O)=O

Technology Process of 10-Methylacridinium Perchlorate

There total 20 articles about 10-Methylacridinium Perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-methyl-2-(10-methyl-9,10-dihydro-acridin-9-yl)-propionic acid methyl ester (24173-45-3) → Methyl isobutyrate (547-63-7,133320-07-7,67505-84-4) + 10-methylacridinium perchlorate (26456-05-3)

Guidance literature:

With perchloric acid; In acetonitrile; at 24.9 ℃; for 10h; Product distribution; other 10-metyhyl-9-alkyl-9,10-dihydroacridines, var. electrophilic reagents, var. times;

DOI:10.1246/cl.1992.1701

Reference yield: 87.0%

dimethyl sulfoxide (67-68-5,8070-53-9) → dimethylsulfide (75-18-3) + 10-methylacridinium perchlorate (26456-05-3)

Guidance literature:

With perchloric acid; 9,10-dihydro-10-methylacridine; water; In acetonitrile; at 24.9 ℃; for 20h; Quantum yield; Mechanism; Irradiation; other sulfoxides; also with AcrD₂;

DOI:10.1021/j100117a018

Reference yield: 86.0%

9-(1-naphthylmethyl)-10-methyl-9,10-dihydroacridine (138616-15-6) → 10-methylacridinium perchlorate (26456-05-3) + 1-Methylnaphthalene (90-12-0,34475-76-8)

Guidance literature:

With perchloric acid; In water; acetonitrile; at 24.9 ℃; for 40h; Quantum yield; Mechanism; Irradiation;

DOI:10.1246/cl.1991.1905

upstream raw materials:

9,10-dihydro-10-methylacridine

1-benzyl-3-cyanoquinolinium perchlorate

9,10-Dihydro-9-isopropyl-10-methylacridine

2-methyl-2-(10-methyl-9,10-dihydro-acridin-9-yl)-propionic acid methyl ester

Downstream raw materials:

9,10-dihydro-10-methylacridine

10-methyl-9, 10-dihydro-9-acridinone

benzaldehyde

Trimethylsilanol