4,4'-bis(4,6-diphenyl-1,3,5-triazin-2-yl)biphenyl

Base Information

• Chemical Name: 4,4'-bis(4,6-diphenyl-1,3,5-triazin-2-yl)biphenyl
• CAS No.: 266349-83-1
• Molecular Formula: C42H28N6
• Molecular Weight: 616.71200
• Mol file: 266349-83-1.mol

Synonyms:2,2'-[1,1'-Biphenyl]-4,4'-diylbis[4,6-diphenyl-1,3,5-triazine];1,3,5-Triazine, 2,2'-[1,1'-biphenyl]-4,4'-diylbis[4,6-diphenyl-;

Chemical Property of 4,4'-bis(4,6-diphenyl-1,3,5-triazin-2-yl)biphenyl

Chemical Property:

• Melting Point: 362℃
• Boiling Point: 878.2±75.0 °C(Predicted)
• PKA: 0.89±0.10(Predicted)
• PSA: 77.34000
• Density: 1.219
• LogP: 9.72560

Purity/Quality:

97% ^*data from raw suppliers

4,4'-Bis(4,6-diphenyl-1,3,5-triazin-2-yl)biphenyl (This product is unavailable in the U.S.) >95.0%(HPLC)(N) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Description: BTB, a triazine compound, namely?4,4'-bis(4,6-diphenyl-1,3,5-triazin-2-yl)biphenyl,?is?used as an electron-transport material in organic light-emitting devices (OLEDs) due to its electron deficiency from the two triazine units.

Technology Process of 4,4'-bis(4,6-diphenyl-1,3,5-triazin-2-yl)biphenyl

There total 2 articles about 4,4'-bis(4,6-diphenyl-1,3,5-triazin-2-yl)biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

→ 4,4’-bis(4,6-diphenyl-1,3,5-triazin-2-yl)biphenyl (266349-83-1)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; water; at 70 ℃; for 12h; Inert atmosphere;

Reference yield: 18.0%

benzonitrile (100-47-0) + 4,4'-biphenyldicarboxylic acid dichloride (2351-37-3) → 4,4’-bis(4,6-diphenyl-1,3,5-triazin-2-yl)biphenyl (266349-83-1)

Guidance literature:

benzonitrile; 4,4'-biphenyldicarboxylic acid dichloride; With aluminum (III) chloride; thionyl chloride; In 1,2-dichloro-benzene; at 150 ℃; for 0.5h; Inert atmosphere;

With ammonium chloride; In 1,2-dichloro-benzene; at 120 - 170 ℃; for 4h;

upstream raw materials:

benzonitrile

4,4'-biphenyldicarboxylic acid dichloride