4-Chloro-2-(prop-2-en-1-yl)aniline

Base Information

Chemical Name:4-Chloro-2-(prop-2-en-1-yl)aniline
CAS No.:267002-56-2
Molecular Formula:C9H10ClN
Molecular Weight:167.638
Hs Code.:
DSSTox Substance ID:DTXSID70583077
Nikkaji Number:J1.291.404K
Wikidata:Q82474593

Synonyms:267002-56-2;4-Chloro-2-(prop-2-en-1-yl)aniline;SCHEMBL21546530;DTXSID70583077

Suppliers and Price of 4-Chloro-2-(prop-2-en-1-yl)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 4-Chloro-2-(prop-2-en-1-yl)aniline

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:167.0501770
Heavy Atom Count:11
Complexity:136

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCC1=C(C=CC(=C1)Cl)N

Technology Process of 4-Chloro-2-(prop-2-en-1-yl)aniline

There total 6 articles about 4-Chloro-2-(prop-2-en-1-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 13519-80-7
N-allyl-4-chloroaniline

: 267002-56-2
4-chloro-2-(prop-2-en-1-yl)aniline

Guidance literature:: With boron trifluoride diethyl etherate; In chlorobenzene; for 6h; Reflux;
DOI:10.1016/j.tetlet.2011.12.095

Reference yield:

: 106-47-8
4-chloro-aniline

: 267002-56-2
4-chloro-2-(prop-2-en-1-yl)aniline

Guidance literature:: Multi-step reaction with 4 steps

1.1: Et₃N / tetrahydrofuran / 14 h / 20 °C

2.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

2.2: tetrahydrofuran / 16 h / Heating

3.1: aq. HCl / tetrahydrofuran / 16 h / Heating

4.1: 67 percent / BF₃*OEt₂ / 17 h / 180 °C

With hydrogenchloride; boron trifluoride diethyl etherate; sodium hydride; triethylamine; In tetrahydrofuran;
DOI:10.1021/ja060291x

Reference yield:

: allyl-(4-chloro-phenyl)-carbamic acid tert-butyl ester

: 267002-56-2
4-chloro-2-(prop-2-en-1-yl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / tetrahydrofuran / 16 h / Heating

2: 67 percent / BF₃*OEt₂ / 17 h / 180 °C

With hydrogenchloride; boron trifluoride diethyl etherate; In tetrahydrofuran;
DOI:10.1021/ja060291x