1-Propanone, 3-(4-chlorophenyl)-1-(2,5-dihydroxyphenyl)-

Base Information

Chemical Name:1-Propanone, 3-(4-chlorophenyl)-1-(2,5-dihydroxyphenyl)-
CAS No.:267885-46-1
Molecular Formula:C15H13ClO3
Molecular Weight:276.719
Hs Code.:

Synonyms:

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Chemical Property of 1-Propanone, 3-(4-chlorophenyl)-1-(2,5-dihydroxyphenyl)-

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Technology Process of 1-Propanone, 3-(4-chlorophenyl)-1-(2,5-dihydroxyphenyl)-

There total 5 articles about 1-Propanone, 3-(4-chlorophenyl)-1-(2,5-dihydroxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 204703-66-2
2',5'-dihydroxy-4-chlorochalcone

: 267885-46-1
2',5'-dihydroxy-4-chlorodihydrochalcone

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 3h; in autoclave;
DOI:10.1211/0022357001773814

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 267885-46-1
2',5'-dihydroxy-4-chlorodihydrochalcone

Guidance literature:: Multi-step reaction with 3 steps

1: barium hydroxide octahydrate / 40 °C

2: 4.29 g / p-toluenesulfonic acid / 20 °C

3: 2.76 g / H₂ / Pd/C / ethyl acetate / 3 h / 20 °C

With barium hydroxide octahydrate; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In ethyl acetate; 1: Claisen-Schmidt condensation;
DOI:10.1016/j.ejmech.2004.09.006

Reference yield:

: 490-78-8
2,5-Dihydroxyacetophenone

: 267885-46-1
2',5'-dihydroxy-4-chlorodihydrochalcone

Guidance literature:: Multi-step reaction with 4 steps

1: pyridium p-toluenesulfonate / 20 °C

2: barium hydroxide octahydrate / 40 °C

3: 4.29 g / p-toluenesulfonic acid / 20 °C

4: 2.76 g / H₂ / Pd/C / ethyl acetate / 3 h / 20 °C

With pyridium para-toluenesulfonate; barium hydroxide octahydrate; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In ethyl acetate; 2: Claisen-Schmidt condensation;
DOI:10.1016/j.ejmech.2004.09.006