Benzenebutanol, b-phenyl-

Base Information

• Chemical Name: Benzenebutanol, b-phenyl-
• CAS No.: 27041-03-8
• Molecular Formula: C16H18O
• Molecular Weight: 226.318
• Mol file: 27041-03-8.mol

Synonyms:4-Hydroxy-1.3-diphenyl-butan;rac.-2,4-Diphenyl-butan-1-ol;4-hydroxy-1.3-diphenyl-butane;(+-)-2,4-diphenyl-butan-1-ol;(R)-2,4-Diphenyl-butan-1-ol;

Chemical Property of Benzenebutanol, b-phenyl-

Chemical Property:

• Boiling Point: 116 - 119 °C (0.01 mmHg)
• PSA: 20.23000
• LogP: 3.39530

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenebutanol, b-phenyl-

There total 12 articles about Benzenebutanol, b-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,4-Diphenyl-3-butin-1-ol (86100-15-4) → 2,4-diphenyl-1-butanol (27041-03-8)

Guidance literature:

With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; under 7600.51 Torr;

DOI:10.1021/acs.orglett.8b02954

Reference yield: 83.0%

(E)-S-ethyl 2,4-diphenylbut-2-enethioate → 2,4-diphenyl-1-butanol (27041-03-8)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃;

DOI:10.1002/adsc.201600623

Reference yield: 80.0%

1,2-epoxy-2,4-diphenylbutane (123200-68-0) → 2,4-diphenyl-1-butanol (27041-03-8)

Guidance literature:

With 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; magnesium bis(trifluoromethane solfonyl)imide; In tetrahydrofuran; at 40 ℃; for 24h; regioselective reaction;

DOI:10.1021/jacs.0c05917

upstream raw materials:

2,4-Diphenyl-3-butin-1-ol

styrene oxide

1-Ethylthio-2-phenyl-acetylen

1,2-epoxy-2,4-diphenylbutane

Downstream raw materials:

racem-2,4-Diphenyl-butyltosylat