Cyclohexanol, 5-methyl-2-(1-methylethyl)-, potassium salt, (1R,2S,5R)-

Base Information

• Chemical Name: Cyclohexanol, 5-methyl-2-(1-methylethyl)-, potassium salt, (1R,2S,5R)-
• CAS No.: 27303-98-6
• Molecular Formula: C10H20O.K
• Molecular Weight: 194.359
• Mol file: 27303-98-6.mol

Synonyms:

Chemical Property of Cyclohexanol, 5-methyl-2-(1-methylethyl)-, potassium salt, (1R,2S,5R)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cyclohexanol, 5-methyl-2-(1-methylethyl)-, potassium salt, (1R,2S,5R)-

There total 2 articles about Cyclohexanol, 5-methyl-2-(1-methylethyl)-, potassium salt, (1R,2S,5R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(-)-menthol (2216-51-5) → potassium (-)-menthoxide (27303-98-6)

Guidance literature:

With potassium hydride; at 20 - 50 ℃; for 5h;

Reference yield:

(-)-menthol (2216-51-5) → potassium (-)-menthoxide (27303-98-6)

Guidance literature:

at 150 ℃; anschliessendes Eindampfen;

DOI:10.1039/jr9310001929

Reference yield: 90.0%

10-bromo-5H-dibenzo[a,d]cyclohepten-5-one (17044-50-7) + potassium (-)-menthoxide (27303-98-6) → 10-[(1R)-menthyloxy]-dibenzo[a,d]cyclohepten-5-one (540512-16-1)

Guidance literature:

In 1,4-dioxane; at 100 ℃; for 3h;

DOI:10.1002/chem.200400441

upstream raw materials:

(-)-menthol

Downstream raw materials:

10-[(1R)-menthyloxy]-dibenzo[a,d]cyclohepten-5-one

5-chloro-10-(2-isopropyl-5-methyl-cyclohexyloxy)-5H-dibenzo[a,d]cycloheptene

(5R/S)-10-[(1R)-menthyloxy]-5H-dibenzo[a,d]cyclohepten-5-ol