Naphthalene, 1-(3-methoxyphenyl)-

Base Information

• Chemical Name: Naphthalene, 1-(3-methoxyphenyl)-
• CAS No.: 27331-43-7
• Molecular Formula: C17H14O
• Molecular Weight: 234.298
• Mol file: 27331-43-7.mol

Synonyms:

Chemical Property of Naphthalene, 1-(3-methoxyphenyl)-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Naphthalene, 1-(3-methoxyphenyl)-

There total 34 articles about Naphthalene, 1-(3-methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-methoxyphenyl bromide (2398-37-0) + 1-Naphthylboronic acid (13922-41-3) → 1-(3-methoxybiphenyl)naphthalene (27331-43-7)

Guidance literature:

With potassium fluoride; monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 1,4-dioxane; at 100 ℃; for 18h;

DOI:10.1021/jo025732j

Reference yield: 98.0%

1-naphthyl mesylate (38262-42-9) + potassium 3-methoxyphenyltrifluoroborate → 1-(3-methoxybiphenyl)naphthalene (27331-43-7)

Guidance literature:

With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; potassium phosphate; tricyclohexylphosphine tetrafluoroborate; In water; tert-butyl alcohol; at 110 ℃; for 4h; Inert atmosphere;

DOI:10.1021/ol101592r

Reference yield: 95.0%

1-chloro-3-methoxy-benzene (2845-89-8) + C12H13OS(1-)*Na(1+) → 1-(3-methoxybiphenyl)naphthalene (27331-43-7)

Guidance literature:

With η³-1-tert-butylindenyl palladium chloride dimer; In toluene; at 70 ℃; for 4h; Inert atmosphere; Glovebox; Sealed tube;

DOI:10.1021/acs.orglett.6b02330

upstream raw materials:

(3-methoxyphenyl)magnesium bromide

3,4-dihydronaphthalene-1(2H)-one

1-Iodonaphthalene

(difluoro)(3-methoxyphenyl)(n-propyl)silane