Phosphonium, bis(3-methyl-2-butenyl)diphenyl-, bromide

Base Information

Chemical Name:Phosphonium, bis(3-methyl-2-butenyl)diphenyl-, bromide
CAS No.:27387-41-3
Molecular Formula:C22H28P.Br
Molecular Weight:403.342
Hs Code.:
DSSTox Substance ID:DTXSID90457807

Synonyms:Phosphonium, bis(3-methyl-2-butenyl)diphenyl-, bromide;27387-41-3;SCHEMBL7742043;DTXSID90457807

Suppliers and Price of Phosphonium, bis(3-methyl-2-butenyl)diphenyl-, bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphonium, bis(3-methyl-2-butenyl)diphenyl-, bromide

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:6
Exact Mass:402.11120
Heavy Atom Count:24
Complexity:358

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CC[P+](CC=C(C)C)(C1=CC=CC=C1)C2=CC=CC=C2)C.[Br-]

Technology Process of Phosphonium, bis(3-methyl-2-butenyl)diphenyl-, bromide

There total 2 articles about Phosphonium, bis(3-methyl-2-butenyl)diphenyl-, bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 603-35-0
triphenylphosphine

: 870-63-3
prenyl bromide

: 27387-41-3
bis(3-methyl-2-butenyl)diphenylphosphonium bromide

Guidance literature:: Yield given. Multistep reaction;
DOI:10.1055/s-1988-27751

Reference yield:

: 870-63-3
prenyl bromide

: 829-85-6
diphenylphosphane

: 27387-41-3
bis(3-methyl-2-butenyl)diphenylphosphonium bromide

Guidance literature:: DOI:10.1039/C2970000631b

Reference yield: 96.0%

: C₁₅H₂₀O₃

: 27387-41-3
bis(3-methyl-2-butenyl)diphenylphosphonium bromide

: C₂₀H₂₈O₂

Guidance literature:: bis(3-methyl-2-butenyl)diphenylphosphonium bromide; With potassium tert-butylate; In 1,2-dimethoxyethane; at 0 ℃; for 0.166667h;

C₁₅H₂₀O₃; In 1,2-dimethoxyethane; for 0.5h; stereoselective reaction; Cooling;
DOI:10.1002/anie.201901651