Phenol, 2-(hydrazinomethyl)-

Base Information

Chemical Name:Phenol, 2-(hydrazinomethyl)-
CAS No.:27412-77-7
Molecular Formula:C7H10N2O
Molecular Weight:138.169
Hs Code.:
DSSTox Substance ID:DTXSID90441645
Wikidata:Q82258502

Synonyms:2-(hydrazinylmethyl)phenol;salicylhydrazine;Phenol, 2-(hydrazinomethyl)-;27412-77-7;SCHEMBL5063012;DTXSID90441645;EN300-1839469

Suppliers and Price of Phenol, 2-(hydrazinomethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Phenol, 2-(hydrazinomethyl)-

Chemical Property:

PSA：58.28000
LogP:1.44670
XLogP3:0.2
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:138.079312947
Heavy Atom Count:10
Complexity:97.6

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)CNN)O

Technology Process of Phenol, 2-(hydrazinomethyl)-

There total 5 articles about Phenol, 2-(hydrazinomethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 187806-33-3
(E)-tert-butyl 2-(2-hydroxybenzylidene)hydrazinecarboxylate

: 27412-77-7
N-(2-hydroxybenzyl)hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / 10percent Pd/C / ethyl acetate / 24 h / 2068.6 Torr / Ambient temperature

2: TFA / CH₂Cl₂ / Ambient temperature

With hydrogen; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm960755+

Reference yield:

: 187806-34-4
N'-(2-Hydroxy-benzyl)-hydrazinecarboxylic acid tert-butyl ester

: 27412-77-7
N-(2-hydroxybenzyl)hydrazine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; Ambient temperature;
DOI:10.1021/jm960755+

Reference yield:

: 187806-33-3
N'-[1-(2-Hydroxy-phenyl)-meth-(E)-ylidene]-hydrazinecarboxylic acid tert-butyl ester

: 27412-77-7
N-(2-hydroxybenzyl)hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: Na(OAc)3BH

2: TFA / CH₂Cl₂

With sodium tris(acetoxy)borohydride; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2006.06.086