Methanesulfonic acid, trifluoro-, lead(2+) salt

Base Information

Chemical Name:Methanesulfonic acid, trifluoro-, lead(2+) salt
CAS No.:27607-92-7
Molecular Formula:2CF₃O₃S*Pb
Molecular Weight:505.341
Hs Code.:

Synonyms:

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Chemical Property of Methanesulfonic acid, trifluoro-, lead(2+) salt

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Technology Process of Methanesulfonic acid, trifluoro-, lead(2+) salt

There total 1 articles about Methanesulfonic acid, trifluoro-, lead(2+) salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1493-13-6
trifluorormethanesulfonic acid

: 27607-91-6
Diethylblei-bis-(trifluormethansulfonat)

: 74-85-1
ethene

: 27607-92-7,56328-89-3,135179-19-0
lead(II) triflate

Guidance literature:: byproducts: C2H6; at 90°C;

Reference yield: 30.0%

: [Na(tetrahydrofuran)(x)]⁽¹⁺⁾*PNb(N(neopentyl)(3,5-(methyl)2C₆H₃))3^(1-)

: 27607-92-7,56328-89-3,135179-19-0
lead(II) triflate

: [(μ2:η(3),η(3)-cyclo-PbP2)(Nb(N(neopentyl)(3,5-(methyl)2C6H3))3)2]

Guidance literature:: In tetrahydrofuran; byproducts: Na(O3SCF3); solns. of Nb compd. and Pb(O3SCF3)2 (0.47 equiv.) were frozen sep. in a glove-box cold well, the thawing soln. of Pb(O3SCF3)2 added dropwise over 1 min to the thawing soln. of Nb compd., allowed to warm to room temp., stirred for 30 min; evapd. (vac.) to dryness, the residue extd. with n-pentane, the ext. filtered through celite, the filtrate evapd. (vac.) to dryness, crystd. by storing a satd. soln. ((C2H5)2O) at -35°C for 1-3 d;
DOI:10.1002/anie.200500707

Reference yield: 24.0%

: (CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2^(1-)*K⁽¹⁺⁾=((CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2)K

: 27607-92-7,56328-89-3,135179-19-0
lead(II) triflate

: 1301753-77-4
(CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2^(1-)*Pb⁽²⁺⁾*O₃SCF₃^(1-)*OC₄H₈=((CH₃)3CC₆H₄C(NC₆H₃(CH(CH₃)2)2)2)Pb(O₃SCF₃)(OC₄H₈)

Guidance literature:: In tetrahydrofuran; byproducts: KO3SCF3; under N2; soln. of K compd. in THF added to soln. of Pb compd. in THF at-78°C; warmed slowly to room temp.; stirred overnight; volatiles removed in vac.; extd. into pentane; concd.; crystd. at -30°C overnight;
DOI:10.1021/ic200682p