Methanone, (pentafluorophenyl)[5-[(pentafluorophenyl)-1H-pyrrol-2-ylmethyl]-1H-pyrr ol-2-yl]-

Base Information

• Chemical Name: Methanone, (pentafluorophenyl)[5-[(pentafluorophenyl)-1H-pyrrol-2-ylmethyl]-1H-pyrr ol-2-yl]-
• CAS No.: 276239-18-0
• Molecular Formula: C22H8F10N2O
• Molecular Weight: 506.302
• Mol file: 276239-18-0.mol

Synonyms:

Chemical Property of Methanone, (pentafluorophenyl)[5-[(pentafluorophenyl)-1H-pyrrol-2-ylmethyl]-1H-pyrr ol-2-yl]-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methanone, (pentafluorophenyl)[5-[(pentafluorophenyl)-1H-pyrrol-2-ylmethyl]-1H-pyrr ol-2-yl]-

There total 4 articles about Methanone, (pentafluorophenyl)[5-[(pentafluorophenyl)-1H-pyrrol-2-ylmethyl]-1H-pyrr ol-2-yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

(pentafluorobenzoyl)pyridyl thioester + 5-(pentafluorophenyl)dipyrromethane (167482-91-9) → 1-(pentafluorobenzoyl)-5-(pentafluorophenyl)dipyrromethane (276239-18-0)

Guidance literature:

5-(pentafluorophenyl)dipyrromethane; With methylmagnesium bromide; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere;

(pentafluorobenzoyl)pyridyl thioester; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1039/d1cc00868d

Reference yield: 55.0%

5-(pentafluorophenyl)dipyrromethane (167482-91-9) + S-pyridin-2-yl pentafluorobenzothioate (262267-31-2) → 1-(pentafluorobenzoyl)-5-(pentafluorophenyl)dipyrromethane (276239-18-0)

Guidance literature:

With ethylmagnesium bromide; In tetrahydrofuran; toluene; at -78 ℃; for 0.25h;

DOI:10.1021/jo991942t

Reference yield: 25.0%

pentafluorobenzoylchloride (2251-50-5) + 5-(pentafluorophenyl)dipyrromethane (167482-91-9) → 1-(pentafluorobenzoyl)-5-(pentafluorophenyl)dipyrromethane (276239-18-0) + (((perfluorophenyl)methylene)bis(1H-pyrrole-5,2-diyl))bis((perfluorophenyl)methanone) (307930-64-9)

Guidance literature:

5-(pentafluorophenyl)dipyrromethane; With ethylmagnesium bromide; In toluene; at 20 ℃; for 0.5h;

pentafluorobenzoylchloride; In toluene; at 20 ℃; for 0.166667h;

DOI:10.1021/jo000882k

upstream raw materials:

5-(pentafluorophenyl)dipyrromethane

S-pyridin-2-yl pentafluorobenzothioate

pentafluorobenzoylchloride

Downstream raw materials:

C₂₂H₆F₁₀N₂O

19-bromo-2,3,4,5-tetrahydro-1,3,3-trimethyl-10,15-bis(pentafluorophenyl)bilene-a

{5-[(5-bromo-1H-pyrrol-2-yl)-pentafluorophenyl-methyl]-1H-pyrrol-2-yl}-pentafluorophenyl-methanol