Methanone, (4,5-dichloro-2-methylphenyl)(4-nitrophenyl)-

Base Information

Chemical Name:Methanone, (4,5-dichloro-2-methylphenyl)(4-nitrophenyl)-
CAS No.:280744-28-7
Molecular Formula:C14H9Cl2NO3
Molecular Weight:310.136
Hs Code.:
DSSTox Substance ID:DTXSID60454808
Wikidata:Q82276558
Mol file:280744-28-7.mol

Synonyms:Methanone, (4,5-dichloro-2-methylphenyl)(4-nitrophenyl)-;280744-28-7;DTXSID60454808

Suppliers and Price of Methanone, (4,5-dichloro-2-methylphenyl)(4-nitrophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Methanone, (4,5-dichloro-2-methylphenyl)(4-nitrophenyl)-

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:308.9959485
Heavy Atom Count:20
Complexity:377

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1C(=O)C2=CC=C(C=C2)[N+](=O)[O-])Cl)Cl

Technology Process of Methanone, (4,5-dichloro-2-methylphenyl)(4-nitrophenyl)-

There total 1 articles about Methanone, (4,5-dichloro-2-methylphenyl)(4-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 95-75-0
3,4-Dichlorotoluene

: 122-04-3
4-nitro-benzoyl chloride

: 280744-28-7
3,4-dichloro-2-(4-nitrobenzoyl)toluene

Guidance literature:: With aluminium trichloride; In 1,2-dichloro-ethane; for 5h; Heating;
DOI:10.1002/jhet.5570390520

Reference yield: 42.0%

: 108-24-7
acetic anhydride

: 280744-28-7
3,4-dichloro-2-(4-nitrobenzoyl)toluene

: 280744-30-1
4,5-dichloro-2-(4-nitrobenzoyl)benzaldehyde acylal

Guidance literature:: With chromium(VI) oxide; sulfuric acid; at 0 - 5 ℃; for 4h;
DOI:10.1002/jhet.5570390520

Reference yield:

: 280744-28-7
3,4-dichloro-2-(4-nitrobenzoyl)toluene

: 280744-57-2
6,7-dichloro-4-(4-nitrophenyl)-1,2-dihydrophthalazine

Guidance literature:: Multi-step reaction with 3 steps

1: 42 percent / chromium(VI) oxide; concd. sulfuric acid / 4 h / 0 - 5 °C

2: 91 percent / hydrazine monohydrate / ethanol / 3 h / Heating

3: 87 percent / sodium borohydride / methanol; CHCl₃ / 3 h / 25 °C

With chromium(VI) oxide; sodium tetrahydroborate; sulfuric acid; hydrazine hydrate; In methanol; ethanol; chloroform;
DOI:10.1002/jhet.5570390520