9h-Fluorene-4-carboxamide

Base Information

Chemical Name:9h-Fluorene-4-carboxamide
CAS No.:28322-01-2
Molecular Formula:C₁₄H₁₁NO
Molecular Weight:209.247
Hs Code.:
DSSTox Substance ID:DTXSID90355399
Nikkaji Number:J1.938.411J
Wikidata:Q82134276
ChEMBL ID:CHEMBL3221417
Mol file:28322-01-2.mol

Synonyms:9h-fluorene-4-carboxamide;28322-01-2;CBMicro_026722;Cambridge id 5633885;Oprea1_675640;Oprea1_699019;SCHEMBL4706819;CHEMBL3221417;DTXSID90355399;AKOS003615126;BIM-0026693.P001;AE-641/00661001;SR-01000314324;SR-01000314324-1;5633-88-5

Suppliers and Price of 9h-Fluorene-4-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
9H-FLUORENE-4-CARBOXYLIC ACID AMIDE 95.00%
5MG
$ 503.97

Total 0 raw suppliers

Chemical Property of 9h-Fluorene-4-carboxamide

Chemical Property:

PSA：44.08000
LogP:3.24090
XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:209.084063974
Heavy Atom Count:16
Complexity:289

Purity/Quality:: 9H-FLUORENE-4-CARBOXYLIC ACID AMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2=C(C3=CC=CC=C31)C(=CC=C2)C(=O)N

Technology Process of 9h-Fluorene-4-carboxamide

There total 6 articles about 9h-Fluorene-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 6954-55-8
fluorene-4-carboxylic acid

: 28322-01-2
fluorene-4-carboxamide

Guidance literature:: With phosphorus pentachloride; In 5,5-dimethyl-1,3-cyclohexadiene; for 2h; Reflux;
DOI:10.1039/d0cc01236j

Reference yield:

: 6223-83-2
9-oxo-9H-fluorene-4-carboxylic acid

: 28322-01-2
fluorene-4-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine; potassium hydroxide / diethylene glycol / 3 h / Reflux

2: phosphorus pentachloride / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / Reflux

With phosphorus pentachloride; potassium hydroxide; hydrazine; In 5,5-dimethyl-1,3-cyclohexadiene; diethylene glycol;
DOI:10.1039/d0cc01236j

Reference yield:

: 863305-32-2
diphenic acid

: 28322-01-2
fluorene-4-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 110 - 115 °C

2: hydrazine; potassium hydroxide / diethylene glycol / 3 h / Reflux

3: phosphorus pentachloride / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / Reflux

With phosphorus pentachloride; sulfuric acid; potassium hydroxide; hydrazine; In 5,5-dimethyl-1,3-cyclohexadiene; diethylene glycol;
DOI:10.1039/d0cc01236j