3,3-Dimethyl-3,4-dihydroisoquinoline

Base Information

• Chemical Name: 3,3-Dimethyl-3,4-dihydroisoquinoline
• CAS No.: 28460-55-1
• Molecular Formula: C11H13N
• Molecular Weight: 159.22800
• DSSTox Substance ID: DTXSID80452922
• Nikkaji Number: J1.018.319G
• Wikidata: Q82273824
• Mol file: 28460-55-1.mol

Synonyms:3,3-dimethyl-3,4-dihydroisoquinoline;28460-55-1;3,3-dimethyl-4H-isoquinoline;3,4-Dihydro-3,3-dimethylisoquinoline;SCHEMBL3936710;DTXSID80452922;FXQNTOHRTXRWTM-UHFFFAOYSA-N;3,4-dihydro-3,3-dimethyl isoquinoline;3,4-dihydro-3,3-dimethyl-isoquinoline;Isoquinoline,3,4-dihydro-3,3-dimethyl-;FT-0748855

Chemical Property of 3,3-Dimethyl-3,4-dihydroisoquinoline

Chemical Property:

• Vapor Pressure: 0.036mmHg at 25°C
• Boiling Point: 249.656oC at 760 mmHg
• Flash Point: 96.455oC
• PSA: 12.36000
• Density: 0.99g/cm3
• LogP: 1.87580
• Storage Temp.: Hygroscopic, Refrigerator, under inert atmosphere
• Solubility.: Chloroform (Slightly), Ethyl Acetate (Slightly)
• XLogP3: 1.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 159.104799419
• Heavy Atom Count: 12
• Complexity: 193

Purity/Quality:

99% ^*data from raw suppliers

3,4-Dihydro-3,3-dimethylisoquinoline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(CC2=CC=CC=C2C=N1)C
• Uses: 3,4-Dihydro-3,3-dimethylisoquinoline can be used as reagent/reactant in synthetic preparation and reactivity of hydroisoquinoline-derived oxaziridines.

Technology Process of 3,3-Dimethyl-3,4-dihydroisoquinoline

There total 10 articles about 3,3-Dimethyl-3,4-dihydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3,3-dimethyl-2-tosyl-1,2,3,4-tetrahydroisoquinoline (200631-40-9) → 3,3-dimethyl-3,4-dihydroisoquinoline (28460-55-1)

Guidance literature:

With potassium hydroxide; In methanol; for 17h; Heating;

DOI:10.1021/jo9718004

Reference yield: 90.0%

→ 3,3-dimethyl-3,4-dihydroisoquinoline (28460-55-1)

Guidance literature:

Reference yield: 75.0%

N-(1,1-dimethyl-2-phenyl-ethyl)-formamide (52117-13-2) → 3,3-dimethyl-3,4-dihydroisoquinoline (28460-55-1)

Guidance literature:

N-(1,1-dimethyl-2-phenyl-ethyl)-formamide; With oxalyl dichloride; In dichloromethane;

With iron(III) chloride;

With methanol; sulfuric acid;

DOI:10.1080/00397911.2010.487175

upstream raw materials:

2-Methyl-1-phenyl-2-propanol

potassium cyanide

1-hydrazino-3,3-dimethyl-3,4-dihydroisoquinoline

N-(1,1-dimethyl-2-phenyl-ethyl)-formamide

Downstream raw materials:

3,3-dimethyl-1,2,3,4-tetrahydroisoquinoline

3,3-dimethyl-3,4-dihydroisoquinoline N-oxide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 28460-55-1 3,4-dihydro-3,3-dimethylIsoquinoline

Send

Send

Metric Ton KG G Pound L ML

Send

Send