3H-Pyridazino[4,5-b]indole-1-carboxylic acid, 7-chloro-3-(3-chlorophenyl)-4,5-dihydro-5-methyl-4-oxo-, ethyl ester

Base Information

Chemical Name:3H-Pyridazino[4,5-b]indole-1-carboxylic acid, 7-chloro-3-(3-chlorophenyl)-4,5-dihydro-5-methyl-4-oxo-, ethyl ester
CAS No.:287099-30-3
Molecular Formula:C20H15Cl2N3O3
Molecular Weight:416.263
Hs Code.:
Mol file:287099-30-3.mol

Synonyms:

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Chemical Property of 3H-Pyridazino[4,5-b]indole-1-carboxylic acid, 7-chloro-3-(3-chlorophenyl)-4,5-dihydro-5-methyl-4-oxo-, ethyl ester

Chemical Property:

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Technology Process of 3H-Pyridazino[4,5-b]indole-1-carboxylic acid, 7-chloro-3-(3-chlorophenyl)-4,5-dihydro-5-methyl-4-oxo-, ethyl ester

There total 3 articles about 3H-Pyridazino[4,5-b]indole-1-carboxylic acid, 7-chloro-3-(3-chlorophenyl)-4,5-dihydro-5-methyl-4-oxo-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 220448-61-3
ethyl 6-chloro-2-(ethoxycarbonyl)-1-methyl-α-oxo-1H-indole-3-acetate

: 2312-23-4
m-chlorophenylhydrazine hydrochloride

: 287099-30-3
ethyl 7-chloro-3-(3-chlorophenyl)-5-methyl-4-oxo-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-carboxylate

Guidance literature:: With sodium hydroxide; acetic acid; In water;

Reference yield:

: 43142-81-0
ethyl 6-chloro-1-methyl-1H-indole-2-carboxylate

: 287099-30-3
ethyl 7-chloro-3-(3-chlorophenyl)-5-methyl-4-oxo-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: titanium tetrachloride / 1,2-dichloro-ethane

2: sodium hydroxide; acetic acid / water

With sodium hydroxide; acetic acid; titanium tetrachloride; In water; 1,2-dichloro-ethane;

Reference yield:

: 27034-51-1
ethyl 6-chloro-1H-indole-2-carboxylate

: 287099-30-3
ethyl 7-chloro-3-(3-chlorophenyl)-5-methyl-4-oxo-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol; water; N,N-dimethyl-formamide

2: titanium tetrachloride / 1,2-dichloro-ethane

3: sodium hydroxide; acetic acid / water

With sodium hydroxide; acetic acid; titanium tetrachloride; In ethanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;