7-Chloro-3-(3-chlorophenyl)-N,N,5-trimethyl-4-oxo-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-carboxamide

Base Information

Chemical Name:7-Chloro-3-(3-chlorophenyl)-N,N,5-trimethyl-4-oxo-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-carboxamide
CAS No.:287099-16-5
Molecular Formula:C₂₀H₁₆Cl₂N₄O₂
Molecular Weight:415.279
Hs Code.:

Synonyms:7-Chloro-3-(3-chlorophenyl)-N,N,5-trimethyl-4-oxo-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-carboxamide

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Chemical Property of 7-Chloro-3-(3-chlorophenyl)-N,N,5-trimethyl-4-oxo-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-carboxamide

Chemical Property:

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Technology Process of 7-Chloro-3-(3-chlorophenyl)-N,N,5-trimethyl-4-oxo-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-carboxamide

There total 3 articles about 7-Chloro-3-(3-chlorophenyl)-N,N,5-trimethyl-4-oxo-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 287099-30-3
ethyl 7-chloro-3-(3-chlorophenyl)-5-methyl-4-oxo-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-carboxylate

: 506-59-2
N,N-dimethylammonium chloride

: 287099-16-5
7-Chloro-3-(3-chlorophenyl)-N,N,5-trimethyl-4-oxo-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-carboxamide

Guidance literature:: With hydrogenchloride; trimethylaluminum; In dichloromethane; water; ethyl acetate; toluene;

Reference yield:

: 43142-81-0
ethyl 6-chloro-1-methyl-1H-indole-2-carboxylate

: 287099-16-5
7-Chloro-3-(3-chlorophenyl)-N,N,5-trimethyl-4-oxo-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: titanium tetrachloride / 1,2-dichloro-ethane

2: sodium hydroxide; acetic acid / water

3: hydrogenchloride / trimethylaluminum / dichloromethane; water; ethyl acetate; toluene

With hydrogenchloride; sodium hydroxide; acetic acid; trimethylaluminum; titanium tetrachloride; In dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; toluene;

Reference yield:

: 27034-51-1
ethyl 6-chloro-1H-indole-2-carboxylate

: 287099-16-5
7-Chloro-3-(3-chlorophenyl)-N,N,5-trimethyl-4-oxo-3,5-dihydro-4H-pyridazino[4,5-b]indole-1-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol; water; N,N-dimethyl-formamide

2: titanium tetrachloride / 1,2-dichloro-ethane

3: sodium hydroxide; acetic acid / water

4: hydrogenchloride / trimethylaluminum / dichloromethane; water; ethyl acetate; toluene

With hydrogenchloride; sodium hydroxide; acetic acid; trimethylaluminum; titanium tetrachloride; In ethanol; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;