1,3-benzodioxol-5-yl(3,4,5-trimethoxyphenyl)methanone

Base Information

Chemical Name:1,3-benzodioxol-5-yl(3,4,5-trimethoxyphenyl)methanone
CAS No.:6327-54-4
Molecular Formula:C₁₇H₁₆O₆
Molecular Weight:316.31
Hs Code.:

Synonyms:Benzophenone,3,4,5-trimethoxy-3',4'-(methylenedioxy)- (6CI,7CI); Methanone,(1,3-benzodioxol-5-yl)(3,4,5-trimethoxyphenyl)- (9CI); NSC 50869

Suppliers and Price of 1,3-benzodioxol-5-yl(3,4,5-trimethoxyphenyl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 1,3-benzodioxol-5-yl(3,4,5-trimethoxyphenyl)methanone

Chemical Property:

Vapor Pressure:1.04E-09mmHg at 25°C
Boiling Point:489°C at 760 mmHg
Flash Point:217.8°C
Density:1.261g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-benzodioxol-5-yl(3,4,5-trimethoxyphenyl)methanone

There total 7 articles about 1,3-benzodioxol-5-yl(3,4,5-trimethoxyphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94-53-1
Piperonylic acid

: 6327-54-4
benzo[1,3]dioxol-5-yl-(3,4,5-trimethoxy-phenyl)-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / CHCl₃ / Heating

2: toluene / Ambient temperature

3: 1.) t-BuLi / 1.) THF, -78 deg C, 15 min, 2.) THF, from -78 to -65 deg C, 4 h

With thionyl chloride; tert.-butyl lithium; In chloroform; toluene;
DOI:10.1021/jm970644q

Reference yield:

: 25054-53-9
3,4-(methylenedioxy)benzoyl chloride

: 6327-54-4
benzo[1,3]dioxol-5-yl-(3,4,5-trimethoxy-phenyl)-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / Ambient temperature

2: 1.) t-BuLi / 1.) THF, -78 deg C, 15 min, 2.) THF, from -78 to -65 deg C, 4 h

With tert.-butyl lithium; In toluene;
DOI:10.1021/jm970644q

Reference yield:

: 63916-59-6
benzo[d][1,3]dioxol-5-yl(morpholino)methanone

: 2675-79-8
1-bromo-3,4,5-trimethoxybenzene

: 6327-54-4
benzo[1,3]dioxol-5-yl-(3,4,5-trimethoxy-phenyl)-methanone

Guidance literature:: With tert.-butyl lithium; Yield given. Multistep reaction; 1.) THF, -78 deg C, 15 min, 2.) THF, from -78 to -65 deg C, 4 h;
DOI:10.1021/jm970644q