10554-32-2Relevant academic research and scientific papers
Microwave-assisted synthesis of 2-substituted 4,5,6,7-tetrahydro-1,3-thiazepines from 4-aminobutanol
Bisceglia, Juan A.,Kilimciler, Natalia B.,Mollo, María C.,Orelli, Liliana R.
, p. 32 - 38 (2020)
A general procedure for the synthesis of 2-substituted tetrahydro-1,3-thiazepines by MW-assisted cyclization of 4-thioamidobutanols is presented. The acyclic precursors were prepared in high overall yields by an expeditious three-step diacylation/thionati
Synthesis of oxazines and thiazines by cyclodehydration of hydroxy amides and thioamides
Wipf, Peter,Hayes, Gregory B.
, p. 6987 - 6998 (2007/10/03)
Dihydro-1,3-oxazines and -thiazines were obtained by cyclodehydration of hydroxy amides and thioamides with PEG-linked Burgess reagent or under Mitsunobu conditions. Yields were generally higher with polymer-Burgess reagent, but both conditions failed to
