106181-25-3Relevant academic research and scientific papers
Highly regioselective lithiation of inter-ring carbon of bis(thien-2yl)methane: a general meso-elaboration protocol
Singh, Kamaljit,Sharma, Amit
experimental part, p. 3682 - 3686 (2010/07/04)
Bis(thien-2yl)methane is regioselectively lithiated at the inter-ring methylene carbon using dimsyl anion in THF at 0 °C; quenching with appropriate electrophile furnishes meso-elaborated derivatives, exclusively with synthetic advantage.
SYNTHESIS OF 16-(4-IODOPHENYL)HEXADECANOIC ACID
Protiva, Jiri,Pecka, Jaroslav,Klinotova, Eva,Prochazka, Milos
, p. 872 - 878 (2007/10/02)
16-(4-Iodophenyl)hexadecanoic acid was prepared in six steps by two methods: from 6-(2-thienyl)hexanoic acid and 6-phenylhexanoyl chloride or by alkylation, or acylation, of 2-thienylthiophene.Mass and 1H NMR spectra of some prepared compounds are discussed.The synthesis is suitable for preparation of radioactively labelled acids used as myocardial imaging agents.
