106543-70-8Relevant academic research and scientific papers
A Further Unsuccessful Effort to Prepare Tetra-tert-butylethene
Dannheim, Joerg,Grahn, Walter,Hopf, Henning,Parrodi, Cecilia
, p. 871 - 872 (2007/10/02)
Rather than providing the title compound 5 the reaction of tetraacetylethene (3) with excess dimethyltitanium dichloride (4) leads to 2,2,4,4,6,6,8,8-octamethyl-3,7-dioxabicyclooct-1(5)-ene (10).The mechanism of formation of this tetramethylated product is discussed.
