108162-74-9Relevant articles and documents
Cycloaddition of Alkenyl Sulfide with α,β-Unsaturated Ketone. A Convenient Route to 1-Cyclobutenyl Ketones
Takeda, Takeshi,Fujii, Toshio,Morita, Koichi,Fujiwara, Tooru
, p. 1311 - 1314 (2007/10/02)
2-Phenylthiocyclobutyl ketones were produced by the reaction of alkenyl sulfides with α,β-unsaturated ketones in the presence of AlCl3.The oxidation with MCPBA and the treatment with LDA or KH of the cycloadducts afford the corresponding 1-cyclobutenyl ke