1097201-77-8

Basic information

• Product Name: N-(3-chlorophenyl)-N-tosylbenzamide
• CAS NO: 1097201-77-8
• Molecular Weight: 385.871
• Mol File: 1097201-77-8.mol
• Article Data: 1

Chemical Properties

• CAS DataBase Reference: N-(3-chlorophenyl)-N-tosylbenzamide(CAS DataBase Reference)
• NIST Chemistry Reference: N-(3-chlorophenyl)-N-tosylbenzamide(1097201-77-8)
• EPA Substance Registry System: N-(3-chlorophenyl)-N-tosylbenzamide(1097201-77-8)

Safety Data

• Hazardous Substances Data: 1097201-77-8(Hazardous Substances Data)

Upstream product

• 19377-04-9 N-(3-chlorophenyl)-4-methyl-benzenesulfonamide 
• 98-88-4 benzoyl chloride 

Relevant articles and documents

An efficient method for the synthesis of N-acylsulfonamides: One-pot sulfonylation and acylation of primary arylamines under solvent-free conditions

The preparation of N-acylsulfonamides is described using primary amines, arylsulfonyl chlorides and acyl chlorides. Reaction of primary aryl amines with arylsulfonyl chlorides in the presence of NaHCO3 produced N-arylsulfonamides, which reacted in situ with benzoyl chloride furnishing the corresponding N-benzoyl-N-arylsulfonamides in 72-96% yields. Accordingly, 4-nitrobenzoyl chloride and 3,5-dinitrobenzoyl chloride were used as acylating agents. All the reactions were carried out under solvent-free conditions at room temperature and the products were isolated after simple work-up in high yields and purity.