110920-93-9Relevant academic research and scientific papers
Synthesis and reactions of 3-C-branched-chain analogues of 3,6-anhydrodeoxynojirimycin
Lee, C. Kuan,Jiang, Huixin,Scofield
, p. 49 - 62 (2007/10/03)
The syntheses of 3,6-anhydro-1-deoxy-3-C-ethoxycarbonylmethyl- (4) and 3-C-(2-hydroxyethyl)nojirimycin (5) from 5-azido-6-O-tert-butyldiphenylsilyl-5-deoxy-1,2-O-isopropylidene-α-D- glucofuranose (8) are described. The key intermediate is 5-azido-6-O-tert
Dipent-4-enyl Acetals as Acetalization Agents
Madsen, Robert,Fraser-Reid, Bert
, p. 749 - 750 (2007/10/02)
Dipent-4-enyl acetals, which are conveniently prepared by treating ketones or aldehydes with pent-4-enyl alcohol under standard conditions, readily acetalize diols in acetonitrile solvent, and although neutral promoters such as N-halogenosuccinimides and
Synthesis, reactions, and crystal structure of 5-azido-6-O-benzoyl-3,5-dideoxy-3-fluoro-1,2-O-isopropylidene-α-D-gluc ofuranose
Lee,Jiang,Koh
, p. 99 - 111 (2007/10/02)
5-Bromo-6-O-tert-butyldiphenylsilyl-5-deoxy-1,2-O-isopropylidene-β-L-t alofuranose (7) was obtained by treatment of 3,5-O-benzylidene-6-O-tert-butyldiphenylsilyl-1,2-O-isopropylidene-α-D -glucofuranose (3) with N-bromosuccinimide followed by Zemplen O-dea
An Improvement in the Preparation of Some Carbohydrate Benzylidene Acetals
Ferro, Vito,Mocerino, Mauro,Stick, Robert V.,Tilbrook, D. Matthew G.
, p. 813 - 815 (2007/10/02)
Carbohydrate benzylidene and p-methoxybenzylidene acetals are easily prepared by treatment of various sugar derivatives with either benzaldehyde diethyl acetal or p-methoxybenzaldehyde diethyl acetal, respectively, in refluxing chloroform containing camph
SPECIFIC SYNTHESIS AND STEREOCHEMICAL ASSIGNMENT OF THE DIASTEREOMERIC 3,5-O-BENZYLIDENE-1,2-O-ISOPROPYLIDENE-α-D-GLUCOFURANOSE ISOMERS
Akerfeldt, Karin,Bartlett, Paul A.
, p. 137 - 146 (2007/10/02)
Pyridinium tosylate-catalysed acetal exchange between benzaldehyde dimethyl acetal and 6-O-(tert-butyldiphenylsilyl)-1,2-O-isopropylidene-α-D-glucofuranose was investigated as an alternative to the original procedure of Brigl and Gruener (condensation of
