1165802-31-2Relevant academic research and scientific papers
Preparation method of alpha-carbonyl amide derivatives
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Paragraph 0035-0037, (2019/01/14)
The invention discloses a preparation method of alpha-carbonyl amide derivatives. According to the method, pyridino-aminoimidazole compounds and water are subjected to ring-opening reaction under theaction of an oxidizing agent, meanwhile, oxygen atoms ar
Palladium-catalyzed double carbonylation using near stoichiometric carbon monoxide: Expedient access to substituted 13C2-labeled phenethylamines
Nielsen, Dennis U.,Neumann, Karoline,Taaning, Rolf H.,Lindhardt, Anders T.,Modvig, Amalie,Skrydstrup, Troels
experimental part, p. 6155 - 6165 (2012/09/21)
A novel and general approach for 13C2- and 2H-labeled phenethylamine derivatives has been developed, based on a highly convergent single-step assembly of the carbon skeleton. The efficient incorporation of two carbon-13 isotopes into phenethylamines was accomplished using a palladium-catalyzed double carbonylation of aryl iodides with near stoichiometric carbon monoxide.
