118-60-5Relevant articles and documents
Method for continuously synthesizing isooctyl salicylate in microchannel (by machine translation)
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Paragraph 0022-0027, (2020/01/14)
To the method, salicylic acid and isooctanol are used as a raw material to synthesize the. isooctyl salicylate to the synthesis of isooctyl salicylate in, the microchannel for a short, time in the process of flowing. (by machine translation)
A method for production of salicylic acid isooctyl
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Paragraph 0059-, (2017/04/11)
The invention provides a method for industrially producing ethylhexyl salicylate. The method comprises the steps of esterifying salicylic acid and isooctyl alcohol in an n-heptane solvent under sodium hydrogen sulfate serving as a catalyst to synthesize a coarse ethylhexyl salicylate product, and enabling the salicylic acid conversion rate to be greater than or equal to 99 percent and the isooctyl ether generation amount to be less than 1 percent by controlling the backflow temperature to be 110+/-5 DEG C and the backflow water division time to be 8-10 hours; then performing decompression rectification, effectively separating impurities with different boiling points by controlling the temperature of circulating water of a built-in backflow condenser to obtain a high-purity ethylhexyl salicylate product, wherein the product yield is greater than or equal to 95 percent, and the purity of a product detected by GC (gas chromatography) is greater than or equal to 99.5 percent. The esterifying synthesized catalyst and the non-reacted salicylic acid can be both recycled and directly used for synthesis of the next batch, so that raw materials are saved and the cost are reduced. The synthesis method is reasonable in design, easy to operate and suitable for being popularized and industrialized.
Flavonoid derivative
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, (2008/06/13)
The invention relates to a novel flavonoid derivative, to an extract comprising the flavonoid derivative, to the cosmetic and pharmaceutical use thereof, to preparations comprising the flavonoid derivative or extract, and to a process for the preparation of the flavonoid derivative or extract.