118576-40-2Relevant academic research and scientific papers
Synthesis of Organofluorine Building Blocks. 3. An Electrochemical Preparation and Reaction of Dimethyl 2,3-Bis(2,2,2-trifluoroethyl)succinate
Uneyama, Kenji,Makio, Shinji,Nanbu, Hiromi
, p. 872 - 877 (2007/10/02)
Dimethyl 2,3-bis(2,2,2-trifluoroethyl)succinate (2) was prepared in a 50percent yield by electrochemical oxidation of trifluoroacetic acid (TFA) and methyl acrylate.Electrolysis was conducted in an MeCN-H2O (7:1)-NaOH (0.1 equiv to TFA) system by using pl
