1190372-76-9Relevant articles and documents
Ultrasound-assisted Wittig reaction and synthesis of 5-alkyl- and 5-alkenyl-resorcinols
Wu, Li-Qiang,Yang, Chun-Guang,Yang, Li-Ming,Yang, Li-Juan
experimental part, p. 183 - 185 (2009/11/30)
Some 5-alkyl- and 5-alkenyl-resorcinols were synthesised from commercially available 3,5-bis(benzylo×y)benzaldehyde by ultrasound-assisted Wittig reaction with alkyltriphenyl phosphonium bromides in basic aqueous condition, followed by debenzylation and simultaneously reduction of a double bond of the styrene type with Na/n-BuOH in overall yields of 62-72%.