1245641-06-8Relevant academic research and scientific papers
A novel alkylation procedure using MW irradiation for the synthesis of 1,2,3-trisubstituted 1,4,5,6,7,8-hexahydro-1,3-diazocinium salts from their corresponding 1,2-diaryldiazocines
Ramírez, María A.,Ortiz, Gisela M.,Salerno, Alejandra,Perillo, Isabel A.,Blanco, María M.
scheme or table, p. 1367 - 1369 (2012/04/10)
In this work, we describe the synthesis of a series of 1,2,3- trisubstituted-1,4,5,6,7,8-hexahydro-1,3-diazocinium salts (1) by alkylation of the corresponding 1,2-diaryl-1,4,5,6,7,8-hexahydro-1,3-diazocines (2). Compounds 2 were obtained by ethyl polypho
1,n-Diamines. Part 4: Synthesis of 1-aryl-2-alkyl-1,4,5,6,7,8-hexahydro-1, 3-diazocines
Díaz, Jimena E.,Gruber, Nadia,Orelli, Liliana R.
, p. 6443 - 6445 (2012/01/19)
In this Letter we present the synthesis of hitherto unreported 1-aryl-2-alkyl-1,4,5,6,7,8-hexahydro-1,3-diazocines 1. Cyclic amidines 1 were synthesized by PPSE promoted ring closure of N-acyl-N'-arylpen- tamethylenediamines 2. The cyclodehydration reacti
New synthetic route for selectively substituted 1,n-diamines. Synthesis of N-aryl tetra- and pentamethylenediamines
Ramirez, María A.,Corona, María V.,Blanco, Maria M.,Perillo, Isabel A.,Porcal, Williams,Salerno, Alejandra
experimental part, p. 5000 - 5002 (2011/02/21)
A general procedure for the synthesis of N-aryltetra- and pentamethylenediamines 1 by acid hydrolysis of N-aryl-N'-acylalkylenediamines 2 under microwave irradiation is described. The precursors 2 are obtained by amination of the corresponding N-(x-haloal
