130255-58-2Relevant academic research and scientific papers
Thiatriazoles. VII. 3-Aroxy-1,2,4-dithiazole-5-imids of 5-Amino-1,2,3,4-thiatriazole
Graubaum, H.,Costisella, B.,Ramm, M.,Schulz, D.
, p. 208 - 214 (2007/10/02)
The unstable but isolable 3-aroxy-1,2,4-dithiazole-5-imids (2a-d) has been found on chlorothioformate acylation of 5-amino-1,2,3,4-thiatriazole (1) in acetonitril.Further acylation and nucleophilic displacement reactions gave stable 3-amino-5-acylimino-1,2,4-dithiazoles (6a-c, 7).The structure of the prepared compounds was inferred from their (1)H and (13)C-n.m.r., mass spectra and corroborated by comparison with the data of similar derivatives as well as by chemical means.
