130944-15-9Relevant academic research and scientific papers
Nano polypropylenimine dendrimer (DAB-PPI-G1): As a novel nano basic-polymer catalyst for one-pot synthesis of 2-amino-2-chromene derivatives
Maleki, Behrooz,Sheikh, Safoora
, p. 42997 - 43005 (2015)
The nano polypropylenimine dendrimer (DAB-PPI-G1) Lewis base catalyst was found to be a highly efficient and recoverable catalyst for the rapid and convenient synthesis of 2-amino-2-chromene derivatives through the three-component condensation of aromatic aldehydes, malononitrile or ethyl cyanoacetate and phenols under solvent-free conditions in excellent yields and short reaction times.
Task specific onium salt as soluble support in multicomponent synthesis of 4-aryl-2-amino-3-ethoxycarbonyl-naphthopyrans
Lu, Cuifen,Zhang, Li,Yang, Guichun,Chen, Zuxing
experimental part, p. 2469 - 2473 (2011/10/02)
In this paper was presented an application of task specific onium salt as soluble support in multicomponent synthesis of 2-amino-3-ethoxycarbonyl- naphthopyrans. The starting task-specific onium salt was functionalized in good yield with chloroethyl alcohol, followed by three steps containing esterification, three components reaction and cleavage from onium salt to afford naphthopyrans in 60% -88% overall yields. All of the products were characterized by IR, 1H NMR, 13C NMR and MS techniques. In this paper was presented an application of task specific onium salt as soluble support in multicomponent synthesis of 2-amino-3-ethoxycarbonyl-naphthopyrans. The starting task-specific onium salt was functionalized in good yield with chloroethyl alcohol, followed by three steps containing esterification, three components reaction and cleavage from onium salt to afford naphthopyrans in 60%-88% overall yields. All of the products were characterized by IR, 1H NMR, 13C NMR and MS techniques.
