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13167-36-7

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13167-36-7 Usage

Synthesis Reference(s)

Tetrahedron Letters, 5, p. 1137, 1964 DOI: 10.1002/lipi.19640660210

Check Digit Verification of cas no

The CAS Registry Mumber 13167-36-7 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 1,3,1,6 and 7 respectively; the second part has 2 digits, 3 and 6 respectively.
Calculate Digit Verification of CAS Registry Number 13167-36:
(7*1)+(6*3)+(5*1)+(4*6)+(3*7)+(2*3)+(1*6)=87
87 % 10 = 7
So 13167-36-7 is a valid CAS Registry Number.
InChI:InChI=1/C3H2Cl2O2/c4-1-2(5)3(6)7/h1H,(H,6,7)/b2-1-

13167-36-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 14, 2017

Revision Date: Aug 14, 2017

1.Identification

1.1 GHS Product identifier

Product name Acrylic acid, .α.-.β.-dichloro-

1.2 Other means of identification

Product number -
Other names 2-Propenoic acid, 2,3-dichloro-

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:13167-36-7 SDS

13167-36-7Downstream Products

13167-36-7Relevant articles and documents

Preparation of (Z)-1,2-dichloroalkenes from terminal alkynes

Zhou, Ningzhang,Wang, Qiang,Lough, Alan J.,Yan, Hongbin

experimental part, p. 625 - 630 (2012/08/08)

(Z)-1,2-Dihaloalkenes are thermodynamically disfavoured of the two stereoisomers. This paper reports the synthesis of some (Z)-1,2-dichloroalkene analogues from mucochloric acid. A more versatile approach involved the chloroboration of terminal alkynes to yield corresponding (Z)-chloroboronic acid as a first step. Treatment of the organoboronic acid with potassium hydrogen difluoride followed by tetrabutylammonium trichloride gave (Z)-1,2- dichloroalkenes in moderate to good yields in a stereospecific manner.

So2-extrusion of an 8-thiabicylo[3.2.1]octa-2,6-diene 8,8-dioxide and rearrangement of the resulting cycloheptatriene

Takayama, Jun,Sugihara, Yoshiaki,Nakayama, Juzo

, p. 132 - 137 (2007/10/03)

The reaction of 3,4-di-tert-butylthio-phene 1-oxide (8) with tetrachlorocyclopropene provided 6,7-di-tert-butyl-2,3,4,4-tetrachloro-8-thia- bicylo[3.2.1]-octa-2,6-diene 8-oxide (10), which was oxidized to the corresponding 8,8-dioxide 16 by m-chloroperbenzoic acid. The thermolysis of 16 in refluxing chlorobenzene, xylene, or octane gave 5-tert-butyl-1,2-dichloro-3- [(1,1-dichloro-2,2-dimethyl)propyl]benzene (18) with extrusion of SO2 and 2-tert-butyl-4,5,6-trichloro-9,9-dimethylbicyclo[5.2.0]nona-1,3,5-triene (19) with extrusion of SO2 and HCl in 73-78% combined yields. On the other hand, the thermolysis of 16 in the presence of triethylamine gave 19 as the sole product in 98% yield. A mechanism that involves the initial formation of 4,5-di-tert-butyl-1,2,7,7-tetrachlorocycloheptatriene (17) is proposed to explain the observed products.

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