1334635-83-4Relevant academic research and scientific papers
A novel approach toward thioester bond formation mediated by N,N’ -diisopropylcarbodiimide in water
Fattahi, Nadia,Varnaseri, Najmeh,Ramazani, Ali
, p. 6 - 12 (2020)
A simple and efficient method has been developed for the synthesis of thioesters from carboxylic acids and thiols using N,N'-diisopropylcarbodiimide (DIC). The reactions were carried out in water as an environmentally friendly and green solvent. The devel
Microwave-assisted Synthesis of Thioesters from Aldehydes and Thiols in Water
Jhuang, Huei-Shu,Liu, Yi-Wei,Reddy, Daggula Mallikarjuna,Tzeng, Yong-Ze,Lin, Wei-Yu,Lee, Chin-Fa
, p. 24 - 27 (2017/10/05)
We describe the synthesis of thioesters via copper- or iron-catalyzed coupling of thiols with aldehydes on application of microwave irradiation. In this protocol, a variety of aliphatic and aromatic aldehydes and thiols were used, and the products were ob
Metal-free cross-coupling reaction of aldehydes with disulfides by using DTBP as an oxidant under solvent-free conditions
Zeng, Jing-Wen,Liu, Yi-Chen,Hsieh, Ping-An,Huang, Yu-Ting,Yi, Chih-Lun,Badsara, Satpal Singh,Lee, Chin-Fa
, p. 2644 - 2652 (2014/05/06)
A DTBP-promoted C-H thiolation of aldehydes with disulfides under metal-free and solvent-free conditions is described. The system shows good functional group tolerance to afford thioesters in moderate to excellent yields. the Partner Organisations 2014.
Synthesis of thioesters through copper-catalyzed coupling of aldehydes with thiols in water
Yi, Chih-Lun,Huang, Yu-Ting,Lee, Chin-Fa
, p. 2476 - 2484 (2013/09/12)
Copper-catalyzed C-S bond formation between aldehydes and thiols in the presence of TBHP as an oxidant is described. Functional groups including chloro, trifluoromethyl, bromo, iodo, nitrile, ester and thiophene are all tolerated by the reaction condition
