134777-64-3Relevant academic research and scientific papers
Synthesis and properties of the salts of 1-nitropropan-2-one and 1-nitrobutan-2-one
Drokin, Roman A.,Rusinov, Vladimir L.,Tiufiakov, Dmitrii V.,Ulomsky, Evgeny N.,Voinkov, Egor K.
, p. 177 - 179 (2020)
A new safe synthesis of α-nitro ketone salts via alkaline hydrolysis of 2-morpholino-1-nitroalkenes has been developed. The salts were introduced into the reactions of diazotization and heterocyclization. Crystal structures of new 2-morpholino-1-nitrobut-1-ene and 6-ethyl-5-nitro-4phenyl-3,4-dihydropyrimidin-2-one have been determined.
