1386972-53-7

Upstream product

• 1383446-30-7 thiotolyl 3-O-acetyl-2-azido-4-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-β-D-glucopyranoside 
• 1386972-44-6 C₂₂H₂₅N₃O₅S 
• 108-24-7 acetic anhydride 
• 220645-79-4 p-methylphenyl 2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside 
• 31505-45-0 2-deoxy-2-phthalimido-β-D-glucopyranose 
• 172847-90-4 p-methylphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside 
• 14131-63-6 D-glucosamine hydrochloride 

Downstream Products

• 1386972-56-0 2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-2-(trichloroethylcarbonylamino)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside 

Relevant academic research and scientific papers

Solid-phase synthesis of 2-aminoethyl glucosamine sulfoforms

Mono- and disaccharides of sulfonated glucosamines (GlcN sulfoforms) conjugated to 2-aminoethyl linkers were generated by solid-phase synthesis. Orthogonally protected intermediates were tethered onto tritylated polystyrene resin beads, subjected to amodular sequence of deprotection and sulfonation steps, then cleaved from solid support without degradation of N- or O-sulfate esters using solvolytic conditions, and finally purified by reverse-phase HPLC to afford the title compounds. Copyright Taylor & Francis Group, LLC.