141075-04-9

Basic information

• Product Name: Pyrimidine, 5-(phenylthio)-
• CAS NO: 141075-04-9
• Molecular Formula: C10H8N2S
• Molecular Weight: 188.253
• Mol File: 141075-04-9.mol
• Article Data: 6

Chemical Properties

• CAS DataBase Reference: Pyrimidine, 5-(phenylthio)-(CAS DataBase Reference)
• NIST Chemistry Reference: Pyrimidine, 5-(phenylthio)-(141075-04-9)
• EPA Substance Registry System: Pyrimidine, 5-(phenylthio)-(141075-04-9)

Safety Data

• Hazardous Substances Data: 141075-04-9(Hazardous Substances Data)

Upstream product

• 4595-59-9 5-bromopyrimidine 
• 882-33-7 diphenyldisulfane 
• 930-69-8 sodium thiophenolate 
• 591-50-4 iodobenzene 
• 17314-33-9 tributyltin phenyl sulfide 

Relevant articles and documents

SINGLE-STEP SYNTHESIS METHOD OF ARYL THIOL AND APPLICATION THEREOF

The present invention relates to a single-step synthesis method of aryl thiol, and more specifically, to a method of synthesizing aryl thiol in a single-step by making aryl halide react with alkane dithiol in the presence of a transition metal catalyst. According to the present invention, a single-step synthesis method using the transition metal catalyst, the synthesis method which is capable of synthesizing aryl thiol from aryl halide at a high yield, can be provided. Various aryl halides may be applied to the synthesis method. Further, the synthesis method has advantages that an easily usable reagent may be used, operations are simple, and reactions can be performed under mild conditions. In addition, the synthesized aryl thiol may be used in the synthesis of advanced molecules such as diaryl sulfides and benzothiophenes.COPYRIGHT KIPO 2017

One-pot synthesis of symmetrical and unsymmetrical aryl sulfides by Pd-catalyzed couplings of aryl halides and thioacetates

Aryl sulfides were obtained from the coupling reaction of S-aryl (or S-alkyl) thioacetates and aryl bromides in the presence of palladium catalyst. This reaction method enables the one-pot synthesis of symmetrical and unsymmetrical diaryl sulfides by employing potassium thioacetate with aryl iodides and aryl bromides.

Syntheses in the nitrogen π-deficient heterocycles series using a barbier type reaction under sonication. Diazines. Part 29

Barbier type reaction with lithium metal has been tested under sonication on pyridines, a cinnoline and on various diazines. This very convenient method allows a very fast and smooth functionalization of these heterocycles. (C) 2000 Elsevier Science Ltd.