1414944-12-9Relevant academic research and scientific papers
Synthesis and characterization of bis-and tris-(4-carboxybenzoyl)- alkaneamines
Guarda,Parra,Chavez,Belmar,Jimenez,Pasan,Ruiz-Perez
, p. 1305 - 1308 (2013/03/28)
A practical and efficient protocol to obtain bis- and tris-(4- carboxybenzoyl)alkaneamines based on monoprotected 1,4-benzenedicarboxylic acid is reported here. N-(4-methoxycarbonylbenzoyloxy)succinimide was treated with aliphatic diamines and triamines to form aliphatic hydrocarbon-linked bis- and tris-amides 4a-4e. The yields ranged from good to very good and showed that choosing the right acylating agent is a key point in this synthesis. All the compounds were characterized by elemental analysis, FTIR, and 1H NMR.
